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Synthesis of Zinc Oxide Nanoparticles and Their Effect on the Compressive Strength and Setting Time of Self-Compacted Concrete Paste as Cementitious Composites

机译:氧化锌纳米粒子的合成及其对自密实水泥糊状水泥浆抗压强度和固化时间的影响

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摘要

In the present study, the mechanical properties of self-compacting concrete were investigated after the addition of different amounts of ZnO nanoparticles. The zinc oxide nanoparticles, with an average particle size of about 30 nm, were synthesized and their properties studied with the help of a scanning electron microscope (SEM) and X-ray diffraction. The prepared nanoparticles were partially added to self-compacting concrete at different concentrations (0.05, 0.1, 0.2, 0.5 and 1.0%), and the mechanical (flexural and split tensile) strength of the specimens measured after 7, 14, 21 and 28 days, respectively. The present results have shown that the ZnO nanoparticles were able to improve the flexural strength of self-compacting concrete. The increased ZnO content of more than 0.2% could increase the flexural strength, and the maximum flexural and split tensile strength was observed after the addition of 0.5% nanoparticles. Finally, ZnO nanoparticles could improve the pore structure of the self-compacted concrete and shift the distributed pores to harmless and less-harmful pores, while increasing mechanical strength.
机译:在本研究中,在添加不同数量的ZnO纳米颗粒后,研究了自密实混凝土的力学性能。合成了平均粒径约为30 nm的氧化锌纳米颗粒,并借助扫描电子显微镜(SEM)和X射线衍射研究了它们的性能。将制备的纳米颗粒以不同的浓度(0.05%,0.1%,0.2%,0.5%和1.0%)部分添加到自密实混凝土中,并在7天,14天,21天和28天后测量样品的机械强度(弯曲和劈裂拉伸强度) , 分别。目前的结果表明,ZnO纳米粒子能够提高自密实混凝土的抗弯强度。 ZnO含量增加超过0.2%可以增加抗弯强度,并且添加0.5%纳米粒子后可以观察到最大的抗弯强度和劈裂强度。最后,ZnO纳米粒子可以改善自密实混凝土的孔结构,并将分布的孔转变为无害和无害的孔,同时提高机械强度。

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